Czasopismo | INŻYNIERIA MATERIAŁOWA | Rocznik 2016 - zeszyt 2

Characterization of IN713C superalloy microstructure after high temperature creep test by LM, SEM and STEM

10.15199/28.2016.2.1

nr katalogowy: 97964
10.15199/28.2016.2.1

This work focuses on the influence of creep phenomenon on the cast IN713C nickel-based superalloy. The carrot-shape IN713C superalloy castings were produced in an investment casting cluster mould and the creep test samples were then prepared from the castings. The creep tests were carried out in order to investigate processing-microstructure-property relationships. The resultant macro- and microstructures were observed and characterized after the creep tests using light microscopy, scanning electron microscopy and scanning transmission electron microscopy. The aim of the analysis was to reveal the changes in the microstructure that occurred as a result of the creep and to identify the phases that participate in voids formation, and crack generation and propagation during the creep tests. It was confirmed that the creep resistance of the IN713C superalloy is negatively affected by some structural characteristics such as porosity, (γ + γ′) eutectic or carbide precipitates along the grain boundaries. Our work confirms that a combination of thermal conditions with a tensile force affected the microstructure of IN713C nickel-based superalloy causing changes in morphologies of the existing precipitations and phase transformations, as in the case of the carbides. Additionally, carbide sulphides containing primarily Zr and intermetallic phase including mainly Ni and Zr were observed. Key words: IN713C, superalloy, creep, microstructure.1. INTRODUCTION Creep, fatigue and the interaction between them play important roles in determining the lifetime of many device components used at elevated temperature. Turbine blades made of nickel-based superalloys are subjected to complex thermal and mechanical creep and fatigue loads [1, 2], resulting in a marked change in microstructure during creep as the originally cubic morphology of the γ′ precipitates becomes directionally coarsened (raft-like) perpendicular to the direction of t[...]

Bibliografia

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