Impulsowo plazmowe spiekanie nanokrystalicznych węglików WC-12Co
Kompozyty WC-Co otrzymywane są poprzez spiekanie węglika wolframu (WC) z ciekłą fazą kobaltu. Spiekanie nanokrystalicznych proszków WC-Co w obecności ciekłej fazy prowadzi jednak do rozrostu ziaren WC[...]
Fe40Al intermetallic samples sintered by pressure-assisted induction sintering (PAIS) method
Low density, high specific strength, high specific stiffness and
enhanced resistance to wear, corrosion of FeAl alloys in
comparison to steels and nickel-based alloys make them attractive
for industrial usage [1, 2]. The mechanical properties of FeAl
alloys highly depends on the aluminum content. For example, the
yield strengths increase with the increase in aluminum content up
to 40 at. % Al [2].
Casting is a traditional method of high-aluminum Fe-Al alloys
manufacturing. However, during the sintering of Fe-Al alloys from
elemental powders strong exothermic reactions (Self propagating
High temperature Synthesis - SHS) take place [3]. This phenomenon
is utilized during reactive casting named the Exo-melt™.
Sikka et al. and Deevi et al. [4÷6] used the exothermic energy
generated in SHS reaction to melt different intermetallics for
casting.
Another method of Fe-Al alloys fabrication is powder
metallurgy (PM). Specimens obtain by the PM method possess
desired geometry, satisfactory mechanical properties and density
close to theoretical.
In the present work, Fe40Al sinters were fabricated from
elemental powders. The pressure-assisted induction sintering
(PAIS) method was used to sinter the specimens. The PAIS
apparatus was built at the Department of Advanced Materials and
Technology of the Military University of Technology and
designed for the production of massive sinters.
APPARATUS
Scheme and an overview of the apparatus for the PAIS is shown in
Figures 1 and 2. The de[...]
The influence of heating rate during sintering on mechanical properties of Fe40Al sinters at room temperature DOI:10.15199/28.2016.5.11
The results of a uniaxial compression test of Fe40Al (at. %) sintered powders are presented. Compression yield stress Rc0.2, ultimate strength Rcm, permanent
deformation, and true compression strength at the maximum force point were determined. All Fe40Al sinters behaved like a plastic material; they were not
brittle, and the sample after the compression test did not fall apart and was barrel-shaped. Observations of the microstructure revealed plastically-deformed
grains. The obtained sinters were characterized by very high ultimate compressive strength (ok. 2700÷2800 MPa) and low yield stress (Rc0.2 approx.
280 MPa). This paper presents also XRD analyses, microstructure, and density of Fe40Al sinters.
Key words: intermetallic alloys, iron aluminides, reaction synthesis, compression test, plasticity.1. INTRODUCTION
Despite its obvious advantages, such as low density, good corrosion
and oxidation resistance, and high strength at both room and
elevated temperature [1÷3], the FeAl-based alloys are still only
potentially used as replacements for expensive alloy steels; this is
primarily due to their ductility and inherently low toughness, especially
at ambient temperature [4]. It is generally known that the
mechanical properties of iron aluminides are very sensitive to many
factors, including aluminium content, order, heat treatment, the test
temperature, alloying additions, environment, microstructure, and
defects [5]. Due to the fragility of Fe-Al alloys, which increases
with increasing aluminium content, alloys with an aluminium content
of 40% are the most frequently analysed. FeAl alloys of 40% Al
are characterized by high strength properties at an acceptable ductility.
Due to the potential embrittlement of sintered FeAl powders, it
is tested mostly by the compression test. Literature sources indicate
that the yield stress of Fe40Al at ambient temperature ranges from
380 to 820 MPa [4, 6÷9]. The strain obtained during testing strength[...]
Functionally graded W-Cu composites produced by the Pulse Plasma Sintering method
The paper presents the results of studies on the fabrication of functionally graded W-Cu composites using the Pulse Plasma Sintering (PPS) method. The functionally graded composites were produced during a single technological process, by sintering powder mixtures with various W/Cu proportions, arranged in consecutive layers. The technological process and the microstructures of the materials [...]